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SECTION IIId.
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SAYBOLT FUROL VISCOSITY @77F (SECONDS) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 1 2 45 37.7 2.5 7.0 6.6 18.6 38.1 2.3 6.6 6.2 17.5 2.1 6.1 5.7 16.0 5.6 15.9 7 8 53 78.6 5.8 16.5 7.4 21.0 76.1 5.9 16.7 7.7 21.9 2.8 8.1 3.6 10.3 3.7 10.6 9 10 29 2273.8 630.5 1783.2 27.7 78.4 3656.7 978.2 2766.7 26.8 75.7 716.6 2026.9 31.5 89.1 19.6 55.4 * 13 14 52 46.7 3.2 8.9 6.8 19.1 45.9 3.3 9.3 7.2 20.2 1.9 5.4 4.1 11.6 4.2 11.8 15 16 51 43.7 2.2 6.3 5.1 14.4 44.3 2.1 5.9 4.7 13.3 1.2 3.3 2.7 7.5 2.6 7.4 17 18 47 14.2 0.7 1.9 4.8 13.6 14.7 0.7 2.0 4.9 13.8 0.4 1.2 3.0 8.5 2.9 8.2 19 20 50 206.8 34.8 98.5 16.8 47.6 207.9 42.0 118.7 20.2 57.1 15.2 42.9 7.3 20.8 7.3 20.7 21 22 72 30.5 1.3 3.7 4.3 12.1 30.5 1.6 4.6 5.3 15.0 0.8 2.3 2.6 7.5 2.6 7.5 23 24 78 28.1 1.4 3.9 4.9 13.8 28.2 1.2 3.5 4.4 12.5 0.7 2.0 2.6 7.3 2.6 7.3 25 26 77 147.6 32.7 92.4 22.1 62.6 123.2 32.9 93.0 26.7 75.5 17.7 50.1 12.0 34.0 14.4 40.7 27 28 85 24.7 1.6 4.5 6.4 18.1 24.5 1.5 4.2 6.1 17.3 0.7 2.1 2.9 8.3 3.0 8.4 29 30 89 25.4 1.8 5.1 7.1 20.2 25.6 1.7 4.8 6.6 18.6 0.8 2.4 3.3 9.3 3.2 9.2 31 32 76 216.6 56.5 159.7 26.1 73.7 218.3 58.1 164.4 26.6 75.3 25.8 72.9 11.9 33.6 11.8 33.4 33 34 92 26.0 1.8 5.0 6.7 19.0 26.5 1.8 5.2 7.0 19.7 1.2 3.4 4.6 12.9 4.5 12.7 35 36 96 33.9 3.1 8.6 9.0 25.5 31.7 2.7 7.7 8.6 24.4 1.7 4.7 4.9 13.9 5.2 14.8Back to Top SAYBOLT FUROL VISCOSITY @122F (SECONDS) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 3 4 48 300.4 54.5 154.1 18.1 51.3 303.8 56.1 158.8 18.5 52.3 26.9 76.1 9.0 25.3 8.9 25.1 5 6 44 154.9 23.7 67.0 15.3 43.2 144.2 23.7 67.1 16.5 46.5 13.8 39.2 8.9 25.3 9.6 27.2 11 12 52 241.3 48.8 138.0 20.2 57.2 229.3 46.8 132.4 20.4 57.8 18.5 52.3 7.7 21.7 8.1 22.8Back to Top DEMULSIBILITY (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 3 4 35 88.5 26.0 73.4 29.3 83.0 88.3 26.9 76.1 30.5 86.2 2.3 6.6 2.6 7.4 2.6 7.5 5 6 35 70.0 16.4 46.5 23.5 66.5 70.0 15.5 43.8 22.1 62.5 3.3 9.5 4.8 13.5 4.8 13.5 19 20 39 45.8 25.4 71.8 55.4 156.8 45.8 25.2 71.4 55.1 155.9 1.0 2.7 2.1 6.0 2.1 6.0 25 26 52 92.9 5.4 15.1 5.8 16.3 91.3 5.9 16.7 6.5 18.3 2.5 7.0 2.7 7.5 2.7 7.6Back to Top CEMENT MIXING (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 7 8 24 0.3 0.4 1.0 113.6 321.4 0.3 0.3 0.8 100.7 284.8 0.1 0.3 33.0 93.4 39.7 112.2 13 14 26 0.1 0.0 0.1 68.6 193.9 0.0 0.0 0.1 84.3 238.4 0.0 0.1 46.9 132.6 71.6 202.4 15 16 24 0.0 0.0 0.1 109.9 310.7 0.0 0.0 0.1 136.6 386.3 0.0 0.1 55.6 157.1 63.2 178.7 17 18 26 0.1 0.1 0.4 88.9 251.3 0.1 0.1 0.4 87.4 247.2 0.0 0.1 31.5 89.2 30.9 87.3 21 22 41 0.1 0.1 0.4 103.5 292.6 0.1 0.1 0.3 97.9 277.0 0.1 0.2 51.6 146.0 58.2 164.6 23 24 38 0.1 0.0 0.1 78.6 222.3 0.1 0.1 0.1 73.0 206.4 0.0 0.1 34.0 96.2 29.5 83.5 27 28 37 0.0 0.0 0.1 98.2 277.6 0.0 0.0 0.1 90.5 255.9 0.0 0.1 63.6 179.9 68.3 193.2Back to Top SIEVE TEST - AMOUNT RET NO. 20 SIEVE (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 1 2 43 0.003 0.006 0.017 186 526 0.004 0.008 0.022 192 543 0.004 0.010 109 310 90 256Back to Top RESIDUE BY DISTILLATION (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 1 2 48 61.7 0.92 2.61 1.5 4.2 61.8 1.00 2.83 1.6 4.6 0.48 1.36 0.78 2.20 0.78 2.20 3 4 47 66.3 0.40 1.14 0.6 1.7 66.1 0.45 1.27 0.7 1.9 0.31 0.89 0.47 1.34 0.48 1.34 5 6 45 64.2 0.43 1.22 0.7 1.9 64.3 0.50 1.41 0.8 2.2 0.29 0.82 0.45 1.27 0.45 1.27 7 8 54 58.9 0.51 1.43 0.9 2.4 58.9 0.45 1.27 0.8 2.2 0.30 0.85 0.51 1.44 0.51 1.44 9 10 41 67.4 0.92 2.59 1.4 3.8 67.4 1.12 3.18 1.7 4.7 0.80 2.27 1.19 3.37 1.19 3.37 11 12 48 68.4 0.43 1.21 0.6 1.8 68.1 0.51 1.45 0.8 2.1 0.33 0.92 0.48 1.35 0.48 1.36 13 14 48 58.4 0.35 0.98 0.6 1.7 58.4 0.41 1.15 0.7 2.0 0.28 0.78 0.47 1.33 0.47 1.33 15 16 47 58.3 0.36 1.02 0.6 1.8 58.3 0.36 1.01 0.6 1.7 0.20 0.56 0.34 0.96 0.34 0.96 17 18 48 56.0 0.59 1.67 1.1 3.0 56.9 0.45 1.27 0.8 2.2 0.37 1.05 0.66 1.87 0.65 1.84 19 20 49 68.4 0.65 1.83 0.9 2.7 68.3 0.73 2.06 1.1 3.0 0.37 1.05 0.54 1.53 0.54 1.53 21 22 74 62.0 0.53 1.49 0.8 2.4 62.1 0.44 1.24 0.7 2.0 0.30 0.85 0.49 1.37 0.48 1.37 23 24 78 63.5 0.36 1.01 0.6 1.6 63.6 0.29 0.81 0.5 1.3 0.19 0.54 0.30 0.84 0.30 0.84 25 26 75 66.8 0.56 1.58 0.8 2.4 66.6 0.49 1.37 0.7 2.1 0.32 0.91 0.48 1.36 0.48 1.37 27 28 84 62.9 0.51 1.44 0.8 2.3 62.8 0.42 1.20 0.7 1.9 0.19 0.52 0.29 0.83 0.29 0.83 29 30 88 62.7 0.55 1.55 0.9 2.5 62.8 0.48 1.35 0.8 2.1 0.36 1.02 0.57 1.62 0.57 1.62 31 32 74 66.3 0.57 1.62 0.9 2.4 66.1 0.52 1.47 0.8 2.2 0.33 0.92 0.49 1.39 0.49 1.39 33 34 92 62.5 0.51 1.44 0.8 2.3 62.8 0.49 1.38 0.8 2.2 0.31 0.89 0.50 1.42 0.50 1.41 35 36 99 66.2 0.51 1.45 0.8 2.2 65.7 0.53 1.49 0.8 2.3 0.35 0.98 0.52 1.48 0.53 1.49Back to Top VOLUME OF OIL DISTILLATE (ML) - RES BY DIST MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 1 2 45 0.56 0.61 1.71 109 308 0.51 0.53 1.49 103 291 0.17 0.47 30 84 32 92 3 4 44 0.35 0.40 1.12 113 319 0.35 0.37 1.04 104 295 0.20 0.57 57 162 57 162 5 6 42 0.67 0.56 1.58 84 237 0.60 0.46 1.30 77 218 0.28 0.78 42 117 47 132 7 8 44 0.43 0.44 1.24 102 288 0.45 0.44 1.25 97 275 0.15 0.43 35 99 33 94 9 10 42 0.94 0.77 2.18 82 232 0.92 0.74 2.09 80 227 0.25 0.70 26 74 27 76 11 12 46 0.34 0.30 0.85 89 251 0.29 0.33 0.92 111 314 0.15 0.41 43 122 50 141 13 14 48 0.54 0.51 1.45 94 266 0.57 0.54 1.54 95 267 0.13 0.38 25 70 23 66 15 16 51 0.70 0.49 1.40 71 200 0.63 0.46 1.31 73 207 0.19 0.53 27 76 30 84 17 18 48 0.63 0.46 1.31 74 208 0.80 0.47 1.33 59 167 0.28 0.80 45 127 35 100 19 20 48 0.27 0.32 0.90 119 336 0.26 0.34 0.95 131 371 0.11 0.32 42 118 44 123 21 22 67 0.55 0.50 1.43 92 261 0.52 0.41 1.16 78 222 0.22 0.61 40 112 41 117 23 24 71 0.34 0.35 0.98 102 290 0.32 0.35 0.99 108 305 0.10 0.29 30 86 32 90 25 26 74 1.26 0.63 1.77 50 140 1.24 0.64 1.80 51 145 0.25 0.71 20 56 20 57 27 28 76 0.51 0.38 1.08 75 211 0.55 0.40 1.14 73 207 0.15 0.42 29 83 27 77 29 30 76 0.57 0.39 1.10 68 191 0.57 0.37 1.05 64 182 0.10 0.28 17 49 17 49 31 32 71 8.66 2.98 8.44 34 98 8.59 3.03 8.56 35 100 0.49 1.37 6 16 6 16 33 34 89 0.41 0.34 0.97 83 236 0.40 0.31 0.87 76 216 0.15 0.43 37 106 38 108 35 36 91 0.44 0.38 1.09 87 246 0.41 0.36 1.01 86 243 0.11 0.32 25 71 27 76Back to Top PENETRATION OF THE RESIDUE (0.1 MM) - RES BY DIST MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 1 2 51 79.1 4.3 12.2 5.4 15.4 79.8 3.5 10.0 4.4 12.5 1.8 5.2 2.3 6.6 2.3 6.5 3 4 50 77.6 3.4 9.7 4.4 12.5 77.2 4.2 11.8 5.4 15.2 1.6 4.6 2.1 6.0 2.1 6.0 5 6 46 131.1 6.1 17.4 4.7 13.2 131.5 5.3 15.0 4.0 11.4 3.7 10.5 2.8 8.0 2.8 8.0 7 8 55 70.6 4.1 11.7 5.9 16.6 70.9 4.3 12.2 6.1 17.2 2.0 5.8 2.9 8.2 2.9 8.1 9 10 44 107.1 13.2 37.3 12.3 34.8 108.8 14.7 41.6 13.5 38.2 5.4 15.3 5.0 14.3 5.0 14.0 11 12 50 121.0 3.6 10.2 3.0 8.4 120.5 4.2 11.8 3.5 9.8 2.7 7.6 2.2 6.3 2.2 6.3 13 14 50 68.4 3.3 9.3 4.8 13.7 68.3 3.7 10.5 5.4 15.4 1.4 3.9 2.0 5.7 2.0 5.7 15 16 52 66.2 2.8 7.9 4.2 12.0 66.0 3.2 9.2 4.9 13.9 1.4 4.1 2.2 6.2 2.2 6.2 17 18 49 94.2 4.1 11.5 4.3 12.2 94.1 4.6 13.1 4.9 13.9 1.8 5.1 1.9 5.4 1.9 5.4 19 20 51 95.0 7.7 21.7 8.1 22.8 94.1 7.6 21.6 8.1 23.0 3.5 9.8 3.6 10.3 3.7 10.4 21 22 77 74.0 7.4 20.9 10.0 28.3 74.4 7.0 19.9 9.5 26.8 2.4 6.7 3.2 9.1 3.2 9.0 25 26 78 123.0 7.4 21.0 6.0 17.0 122.6 6.9 19.6 5.7 16.0 3.3 9.3 2.7 7.5 2.7 7.6 27 28 85 78.4 5.9 16.7 7.5 21.2 79.2 5.8 16.5 7.4 20.8 1.9 5.3 2.4 6.8 2.4 6.7 29 30 88 81.0 5.5 15.7 6.8 19.4 81.4 5.8 16.4 7.1 20.2 2.1 6.1 2.6 7.5 2.6 7.4 31 32 76 119.8 19.2 54.4 16.0 45.4 117.9 20.3 57.5 17.2 48.8 8.3 23.4 6.9 19.5 7.0 19.8 33 34 98 85.0 9.0 25.4 10.5 29.8 86.2 8.0 22.7 9.3 26.3 3.4 9.5 4.0 11.2 3.9 11.0 35 36 98 111.2 8.4 23.9 7.6 21.4 112.7 8.7 24.7 7.8 21.9 4.2 12.0 3.8 10.8 3.8 10.6Back to Top SOLUBILITY OF THE RESIDUE (PERCENT) - RES BY DIST MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 1 2 46 99.33 0.25 0.70 0.25 0.71 99.27 0.26 0.73 0.26 0.74 0.11 0.30 0.11 0.30 0.11 0.30 3 4 41 99.96 0.03 0.07 0.03 0.07 99.96 0.04 0.10 0.04 0.10 0.02 0.05 0.02 0.05 0.02 0.05 * 5 6 40 99.96 0.05 0.13 0.05 0.13 99.96 0.04 0.12 0.04 0.12 0.02 0.05 0.02 0.05 0.02 0.05 7 8 50 98.42 0.81 2.29 0.82 2.33 98.42 0.79 2.23 0.80 2.27 0.41 1.17 0.42 1.19 0.42 1.19 9 10 40 99.42 0.58 1.64 0.58 1.65 99.36 0.56 1.58 0.56 1.59 0.20 0.58 0.21 0.58 0.21 0.58 11 12 43 99.96 0.03 0.07 0.03 0.07 99.96 0.02 0.07 0.02 0.07 0.01 0.03 0.01 0.03 0.01 0.03 13 14 44 98.75 0.72 2.03 0.73 2.06 98.74 0.67 1.89 0.68 1.91 0.24 0.67 0.24 0.68 0.24 0.68 15 16 48 99.03 0.64 1.81 0.65 1.83 98.94 0.61 1.73 0.62 1.75 0.30 0.86 0.31 0.87 0.31 0.87 17 18 46 99.84 0.07 0.20 0.07 0.20 99.84 0.08 0.22 0.08 0.22 0.04 0.11 0.04 0.11 0.04 0.11 19 20 48 99.93 0.07 0.20 0.07 0.20 99.93 0.07 0.19 0.07 0.19 0.04 0.13 0.04 0.13 0.04 0.13 21 22 68 99.19 0.40 1.14 0.41 1.15 99.18 0.40 1.14 0.41 1.15 0.17 0.47 0.17 0.47 0.17 0.47 25 26 57 99.95 0.04 0.11 0.04 0.11 99.95 0.03 0.09 0.03 0.09 0.02 0.07 0.02 0.07 0.02 0.07 27 28 69 99.67 0.12 0.35 0.12 0.35 99.67 0.12 0.34 0.12 0.34 0.06 0.18 0.06 0.18 0.06 0.18 29 30 69 99.68 0.11 0.31 0.11 0.31 99.70 0.13 0.36 0.13 0.36 0.08 0.22 0.08 0.22 0.08 0.22 31 32 56 99.90 0.06 0.17 0.06 0.17 99.91 0.06 0.17 0.06 0.17 0.05 0.13 0.05 0.13 0.05 0.13 33 34 69 99.72 0.11 0.30 0.11 0.30 99.74 0.11 0.31 0.11 0.31 0.06 0.16 0.06 0.16 0.06 0.16 35 36 67 99.69 0.14 0.40 0.14 0.41 99.70 0.15 0.43 0.15 0.43 0.07 0.19 0.07 0.19 0.07 0.19Back to Top FLOAT TEST (SECONDS) - RES BY DIST MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 3 4 33 1204 510 1444 42 120 1332 532 1505 40 113 308 872 26 72 23 65Back to Top RESIDUE BY EVAPORATION (PERCENT) MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 3 4 37 66.4 0.22 0.63 0.3 1.0 66.4 0.27 0.75 0.4 1.1 0.17 0.47 0.25 0.70 0.25 0.70 5 6 34 64.3 0.35 0.98 0.5 1.5 64.4 0.34 0.96 0.5 1.5 0.24 0.69 0.38 1.07 0.38 1.07 7 8 40 59.2 0.21 0.59 0.4 1.0 59.2 0.25 0.70 0.4 1.2 0.18 0.51 0.30 0.85 0.30 0.85 9 10 35 67.6 0.37 1.06 0.6 1.6 67.8 0.55 1.54 0.8 2.3 0.43 1.23 0.64 1.82 0.64 1.81 * 11 12 41 68.4 0.25 0.70 0.4 1.0 68.3 0.49 1.38 0.7 2.0 0.35 0.98 0.50 1.43 0.50 1.43 13 14 41 58.6 0.18 0.52 0.3 0.9 58.6 0.16 0.45 0.3 0.8 0.12 0.34 0.21 0.58 0.21 0.58 15 16 44 58.5 0.21 0.58 0.4 1.0 58.5 0.19 0.54 0.3 0.9 0.13 0.37 0.23 0.64 0.23 0.64 17 18 42 56.3 0.29 0.82 0.5 1.5 57.2 0.27 0.76 0.5 1.3 0.25 0.72 0.45 1.27 0.44 1.25 19 20 40 68.7 0.33 0.93 0.5 1.4 68.7 0.20 0.55 0.3 0.8 0.23 0.64 0.33 0.93 0.33 0.93 21 22 65 62.3 0.29 0.81 0.5 1.3 62.3 0.20 0.55 0.3 0.9 0.19 0.55 0.31 0.88 0.31 0.88 23 24 65 63.6 0.21 0.60 0.3 0.9 63.6 0.22 0.63 0.4 1.0 0.16 0.46 0.25 0.72 0.25 0.72 25 26 62 67.0 0.33 0.93 0.5 1.4 66.9 0.35 1.00 0.5 1.5 0.25 0.72 0.38 1.07 0.38 1.07 27 28 68 63.0 0.45 1.29 0.7 2.0 63.0 0.39 1.10 0.6 1.7 0.24 0.67 0.37 1.06 0.37 1.06 29 30 69 63.1 0.37 1.06 0.6 1.7 63.1 0.26 0.74 0.4 1.2 0.19 0.53 0.30 0.84 0.30 0.85 31 32 64 65.7 0.75 2.12 1.1 3.2 65.5 0.81 2.30 1.2 3.5 0.33 0.93 0.50 1.42 0.50 1.43 33 34 70 62.8 0.38 1.06 0.6 1.7 63.0 0.38 1.09 0.6 1.7 0.25 0.72 0.40 1.15 0.40 1.14 35 36 72 66.5 0.45 1.28 0.7 1.9 65.8 0.47 1.34 0.7 2.0 0.35 1.00 0.53 1.50 0.54 1.52Back to Top PENETRATION OF THE RESIDUE (0.1 MM) - RES BY EVAP MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 3 4 37 72.8 8.0 22.7 11.0 31.1 73.5 8.7 24.5 11.8 33.3 2.9 8.1 3.9 11.2 3.9 11.1 5 6 34 116.1 13.2 37.4 11.4 32.2 116.2 13.3 37.7 11.5 32.4 2.6 7.4 2.2 6.3 2.2 6.3 7 8 40 60.9 5.6 15.8 9.2 26.0 60.2 7.0 19.7 11.6 32.7 2.4 6.9 4.0 11.3 4.0 11.4 9 10 35 101.7 15.6 44.2 15.4 43.5 101.5 18.0 51.0 17.8 50.2 9.2 26.1 9.1 25.7 9.1 25.7 11 12 42 105.8 12.0 34.0 11.3 32.1 105.0 10.9 30.8 10.4 29.4 3.0 8.4 2.8 8.0 2.8 8.0 13 14 44 58.4 6.5 18.4 11.1 31.5 58.1 7.5 21.2 12.9 36.5 1.6 4.6 2.8 7.9 2.8 7.9 15 16 46 56.7 6.4 18.2 11.4 32.2 56.4 6.3 17.9 11.2 31.6 1.5 4.3 2.7 7.6 2.7 7.7 17 18 43 76.2 7.5 21.1 9.8 27.7 76.5 7.9 22.4 10.3 29.2 2.2 6.3 2.9 8.3 2.9 8.2 19 20 42 85.8 7.4 20.8 8.6 24.3 85.4 7.2 20.5 8.5 24.0 2.3 6.4 2.6 7.5 2.6 7.5 21 22 65 63.9 7.0 19.7 10.9 30.8 64.6 7.2 20.4 11.2 31.6 2.4 6.9 3.8 10.8 3.8 10.7 23 24 64 108.8 10.3 29.0 9.4 26.7 109.2 12.3 34.8 11.3 31.9 3.5 9.8 3.2 9.0 3.2 9.0 25 26 66 104.7 12.9 36.6 12.4 35.0 105.0 13.1 36.9 12.4 35.2 4.5 12.8 4.3 12.2 4.3 12.2 27 28 64 66.0 6.0 16.9 9.1 25.6 65.8 6.0 17.0 9.1 25.8 1.8 5.2 2.8 7.9 2.8 7.9 29 30 73 68.7 8.5 24.0 12.3 34.9 68.8 8.4 23.7 12.2 34.5 2.1 5.8 3.0 8.5 3.0 8.5 31 32 62 93.4 28.4 80.2 30.4 85.9 92.3 28.5 80.6 30.9 87.3 12.9 36.4 13.8 39.0 14.0 39.5 33 34 73 70.8 8.0 22.5 11.2 31.8 72.0 8.1 22.9 11.2 31.8 2.9 8.2 4.1 11.6 4.0 11.4 35 36 72 89.3 10.7 30.4 12.0 34.0 90.6 10.9 30.9 12.1 34.1 2.9 8.1 3.2 9.0 3.1 8.9Back to Top SOLUBILITY OF THE RESIDUE (PERCENT) - RES BY EVAP MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 3 4 35 99.91 0.09 0.27 0.09 0.27 99.91 0.07 0.20 0.07 0.20 0.07 0.18 0.07 0.18 0.07 0.18 * 5 6 32 99.96 0.02 0.07 0.02 0.07 99.97 0.03 0.08 0.03 0.08 0.02 0.06 0.02 0.06 0.02 0.06 7 8 41 98.21 1.35 3.81 1.37 3.88 98.25 1.21 3.41 1.23 3.47 0.68 1.93 0.70 1.97 0.70 1.97 9 10 31 99.36 0.58 1.63 0.58 1.64 99.36 0.59 1.66 0.59 1.67 0.30 0.85 0.30 0.85 0.30 0.85 11 12 40 99.96 0.03 0.08 0.03 0.08 99.95 0.04 0.12 0.04 0.12 0.03 0.09 0.03 0.09 0.03 0.09 13 14 41 98.54 1.03 2.92 1.05 2.97 98.70 1.03 2.92 1.05 2.96 0.35 0.99 0.35 1.00 0.35 1.00 15 16 43 99.15 0.78 2.20 0.78 2.22 99.10 0.81 2.28 0.82 2.31 0.26 0.74 0.26 0.75 0.26 0.75 17 18 41 99.82 0.13 0.36 0.13 0.36 99.83 0.11 0.31 0.11 0.31 0.05 0.14 0.05 0.14 0.05 0.14 19 20 39 99.87 0.13 0.38 0.13 0.38 99.89 0.10 0.28 0.10 0.28 0.05 0.13 0.05 0.13 0.05 0.13 21 22 62 99.34 0.47 1.34 0.48 1.35 99.38 0.41 1.15 0.41 1.15 0.18 0.52 0.18 0.52 0.18 0.52 23 24 58 99.33 0.31 0.88 0.31 0.88 99.37 0.30 0.86 0.31 0.86 0.09 0.26 0.09 0.26 0.09 0.26 25 26 53 99.95 0.04 0.11 0.04 0.11 99.94 0.05 0.13 0.05 0.13 0.03 0.08 0.03 0.08 0.03 0.08 27 28 57 99.75 0.12 0.34 0.12 0.34 99.74 0.12 0.33 0.12 0.33 0.06 0.17 0.06 0.17 0.06 0.17 29 30 60 99.74 0.13 0.37 0.13 0.37 99.74 0.13 0.36 0.13 0.37 0.08 0.23 0.08 0.24 0.08 0.24 31 32 51 99.86 0.07 0.19 0.07 0.19 99.85 0.08 0.23 0.08 0.23 0.05 0.14 0.05 0.14 0.05 0.14 33 34 56 99.74 0.11 0.30 0.11 0.30 99.77 0.11 0.30 0.11 0.30 0.05 0.15 0.05 0.15 0.05 0.15 35 36 53 99.68 0.17 0.49 0.17 0.49 99.72 0.16 0.44 0.16 0.44 0.08 0.21 0.08 0.21 0.08 0.21Back to Top FLOAT TEST (SECONDS) - RES BY EVAP MULTILABORATORY PRECISION MULTILABORATORY PRECISION SINGLE-OPERATOR PRECISION SAMPLE NO. 1ST SAMPLE 2ND SAMPLE 1ST SMPL 2ND SMPL NUMBERS LABS AVG 1S D2S 1S% D2S% AVG 1S D2S 1S% D2S% 1S D2S 1S% D2S% 1S% D2S% 3 4 26 700 332 938 47 134 686 318 899 46 131 174 491 25 70 25 72 9 10 5 2916 1643 4648 56 159 3035 2313 6542 76 216 1314 3717 45 128 43 123Back to Top |